File:Widmer orig schematic flows.png

Page contents not supported in other languages.
This is a file from the Wikimedia Commons
From Wikipedia, the free encyclopedia

Original file(169 × 604 pixels, file size: 34 KB, MIME type: image/png)

Summary

Description
English: Widmer column/air condenser, chemical laboratory scale simplified modern representation.

This representation of a research laboratory-scale Widmer column—a complex type of air condenser combining Golodetz-type concentric tubes and a Dufton-type glass rod-and-wound-spiral—was created for pedagogical purposes, based on references 1 and 2 (Widmer 1923 dissertation and publication, supported by various secondary sources such as Krell's 1982 Handbook of Laboratory Distillation, and Armarego's Purification of Lab Chemicals). See the latter for "pro's" and the former for "con's", on the Widmer column.

Changes: Stoppered seal of the original outer dead air space design was modernized to a ring seal, the J-shaped discharge tube was omitted for simplicity of description, and top and bottom ports were converted to appear as tapered ground joints (here, matching a side-by-side appearing Vigreux column from the important earlier image effort of User:YassineMrabet on the Vigreux). Finally, limited numbering and colored arrows were added to streamline legend descriptions in articles. If photographs of Widmer columns ever make their way into Wikimedia Commons, this schematic image should considered complimentary, for ease of explanation. Note, had the Swiss not a 70 year author post partim copyright restriction on reproducing such content, I would have simply uploaded the historically more interesting, and approximately as easily understood original Widmer images. Alas.

[File created from available individual chemistry graphic arts components, by simple editing in GraphicConverter9.] Le Prof

References: 1. Gustav Widmer, 1923, "Über die fraktionierte Destillation kleiner Substanzmengen" [doctoral dissertation], der Eidgenössischen Technischen Hochschule (ETH), Zürich, der Schweiz, approved 1923, DOI 10.3929/ethz-a-000090805, see also [1], accessed 14 February 2015. 2. Gustav Widmer, 1924, "Über die fraktionierte Destillation kleiner Substanzmengen," Helvetica Chimica Acta, 7(1), pp. 59–61, DOI 10.1002/hlca.19240070107, see also [2], accessed 14 February 2015. [Note, the 1927 reference to a related Widmer distillation article in Helv. Chim. Acta appears to be an error on the part of L.P. Kyrides, (see Org. Synth, 1940, 20, pp. 51 ff).]
Date
Source Own work
Author Leprof 7272

Licensing

I, the copyright holder of this work, hereby publish it under the following license:
w:en:Creative Commons
attribution share alike
This file is licensed under the Creative Commons Attribution-Share Alike 4.0 International license.
You are free:
  • to share – to copy, distribute and transmit the work
  • to remix – to adapt the work
Under the following conditions:
  • attribution – You must give appropriate credit, provide a link to the license, and indicate if changes were made. You may do so in any reasonable manner, but not in any way that suggests the licensor endorses you or your use.
  • share alike – If you remix, transform, or build upon the material, you must distribute your contributions under the same or compatible license as the original.

Captions

Add a one-line explanation of what this file represents

Items portrayed in this file

depicts

14 February 2015

File history

Click on a date/time to view the file as it appeared at that time.

Date/TimeThumbnailDimensionsUserComment
current09:35, 14 February 2015Thumbnail for version as of 09:35, 14 February 2015169 × 604 (34 KB)Leprof 7272User created page with UploadWizard
The following pages on the English Wikipedia use this file (pages on other projects are not listed):